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The gradient started with 0.5% solvent B at a flow rate of 0.4 mL/min for 1 min and then ramped up to 95% solvent B at a flow rate of 0.35 mL/min over a period of 3 min

There was a period there where states were allowing children to buy these flavored e-cigarettes, he says

Thanks #2 Welcome to the forum

Thats the opposite of the new paper